期刊
TETRAHEDRON
卷 70, 期 46, 页码 8885-8892出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2014.09.092
关键词
1,2,3-Triazoles; Polymer-supported cryptand-22; Heterogeneous catalysis; Three-component reaction; Terminal alkyne
资金
- K. N. Toosi University of Technology Research Council
Polystyrene resin-supported copper(I) iodide-cryptand-22 complex (PS-C22-CuI) was synthesized and characterized by FT-IR, EDX, SEM, XPS, and TG-DTA analysis. This complex was found to be a highly active and robust heterogeneous catalyst for either three-component reaction of organic halides, sodium azide, and terminal alkynes, or the reaction of organic azides and alkynes to form 1,4-disubstituted 1,2,3-triazoles in good to excellent yields at room temperature, using water as the green solvent. The catalyst can be not only easily isolated from the final product by filtration but also reused without significant loss of catalytic activity. (C) 2014 Elsevier Ltd. All rights reserved.
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