期刊
TETRAHEDRON
卷 69, 期 30, 页码 6213-6218出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2013.05.039
关键词
Helicene; Palladium cross-coupling; Microwave-assisted synthesis
资金
- Grant Agency of the Czech Republic [P207/10/1124]
- Technology Agency of the Czech Republic [TA01010646]
- Ministry of Industry and Trade of the Czech Republic [FR-TI3/628]
Exploration of 9-bromo[7]helicene reactivity mainly in Pd-catalyzed reactions is reported. Palladium catalyzed carbon-carbon and carbon-heteroatom coupling reactions provide a large portfolio of racemic helicenes bearing different functional groups in good to excellent yields. Many of the reactions were performed in the microwave reactor keeping reaction time to a minimum compared with conventional synthetic methods. (C) 2013 Elsevier Ltd. All rights reserved.
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