期刊
TETRAHEDRON
卷 69, 期 1, 页码 160-173出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2012.10.050
关键词
Catalysis; Heck reaction; Palladium; Cyclization; Heterocycles
Benzothiophenes and dibenzothiophenes were prepared by twofold Heck reactions of 2,3-dibromothiophene and 2,3-dibromobenzothiophene, respectively, and subsequent thermal 6 pi-electrocyclization. The Heck reaction of 2,3-dibromothiophene and 2,3-dibromobenzothiophene with 1 equiv of alkenes proceeded with different regioselectivities and afforded 2-alkenylthiophenes and 3-alkenylbenzothiophenes. (C) 2012 Elsevier Ltd. All rights reserved.
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