期刊
TETRAHEDRON
卷 67, 期 2, 页码 383-389出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2010.11.031
关键词
2,5-Diamino-2,5-dideoxy-1,4-3,6-dianhydroiditol; Bio-based; Building blocks; Renewable resources
资金
- Dutch Polymer Institute (DPI), Eindhoven, the Netherlands [653, 656]
An efficient route towards the synthesis of 2,5-diamino-2,5-dideoxy-1,4-3,6-dianhydroiditol 4 has been developed resulting in significant improvements in both isolated yields and purity when compared to literature procedures. As a consequence, resin-grade 2,5-diamino-2,5-dideoxy-1,4-3,6-dianhydroiditol 4 has become available for laboratory scale step-growth polymer synthesis. Additionally, an interesting renewable chiral 2-amino-2-deoxy-1,4-3,6-dianhydroiditol 10, has been isolated. (C) 2010 Elsevier Ltd. All rights reserved.
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