4.4 Article

Scope of AuCl3 in the activation of per-O-acetylglycals

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TETRAHEDRON
卷 65, 期 39, 页码 8139-8142

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PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2009.07.087

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  1. DST, New Delhi

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Gold(III)chloride in catalytic amounts activates 3,4,6-tri-O-acetyl-D-glucal, 3,4,6-tri-O-acetyl-D-galactal, and 3,4-di-O-acetyl-L-rhamnal efficiently. The activated species can be employed in the Ferrier reaction with different nucleophiles at ambient conditions. Attempts have been made to make beta-anomer of the Ferrier product from anomeric-O-propargylated Ferrier product. (C) 2009 Elsevier Ltd. All rights reserved.

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