期刊
TETRAHEDRON
卷 65, 期 25, 页码 4859-4865出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2009.04.034
关键词
Benzobarrelene; Bromination; Benzosemibullvalene; Polybromides; Polychlorides; Polyhalogenides
资金
- TUBITAK [106T658]
- Ataturk University, TUBA [AD/TUBA-GEBIP/2001-1-3]
New polyhalogenated benzobarrelenes were synthesized in good yields. The bromination reaction of benzobarrelenes at high temperature gives non-rearranged products. Dehydrobromination of the formed products with t-BuOK yielded the desired polyhalogenated benzobarrelenes. The elimination reaction of cyclopropanoid dibromide with a base unusually resulted in the formation of a benzosemibullvalene derivative. (C) 2009 Elsevier Ltd. All rights reserved.
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