期刊
TETRAHEDRON
卷 64, 期 46, 页码 10497-10500出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2008.09.005
关键词
Fluorine; Hexafluoropropan-2-ol; Sugar; Glycals
资金
- CEFIPRA/IFCPAR
Hexafluoroisopropanol (HFIP) is explored as an effective medium for the synthesis of 2,3-unsaturated glycosides through allylic rearrangement of 3,4,6-tri-O-acetyl glucal. This metal-free, exclusively solvent-promoted Ferrier glycosylation, affords products in good to excellent yields and with good a-selectivity. (c) 2008 Elsevier Ltd. All rights reserved.
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