期刊
SYNTHETIC COMMUNICATIONS
卷 40, 期 21, 页码 3135-3151出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/00397910903341189
关键词
Azomethine ylide; 1; 3-dipolar cycloaddition; spiropyrrolidine; spiropyrrolizine; triarylideneacetylacetone
Triarylideneacetylacetone undergoes regioselective 1,3-dipolar cycloaddition reactions with azomethine ylide derived from isatin and L-proline/sarcosine/octahydro-1H-indole-2-carboxylic acid by decarboxylation, affording a series of spiroheterocycles. This one-pot, three-component tandem reaction is efficient and yields novel spiroheterocylic compounds in good yields. The structure and stereochemistry of the cycloadduct have been established by single-crystal x-ray and spectroscopic techniques.
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