期刊
SYNTHESIS-STUTTGART
卷 44, 期 14, 页码 2249-2254出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0031-1290444
关键词
ethers; amides; arenes; protecting groups; coupling
资金
- Fonds pour la Recherche Scientifique (F.R.S.-FNRS) of Belgium
- Walloon Government (Belgium)
A modular synthesis of photoactivable cross-linking agents is described, using an aromatic core, di- or triethyleneglycol spacers and photoaffinity labeling synthons that feature either perfluorophenyl azide or aryl(trifluoromethyl)diazirine motifs. Symmetrical and nonsymmetrical trivalent structures were obtained from phloroglucinol and dopamine, respectively. Symmetrical tetravalent structures resulted from the coupling of two dopamine derivatives with oxalyl chloride.
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