期刊
SYNTHESIS-STUTTGART
卷 -, 期 18, 页码 2945-2950出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0030-1260145
关键词
alpha-amino acids; [2+2+2] cycloaddition; indane-based alpha-amino acid; benzocyclobutene; ethyl isocyanoacetate; diversity-oriented approach
资金
- CSIR, New Delhi
- DST
- Department of Chemistry, IIT-Bombay
The benzocyclobutene-based alpha-amino acid derivative, ethyl 5-acetamido-2,4,5,6-tetrahydro-1H-cyclobuta[f] indene-5-carboxylate is synthesized via coupling of a benzocyclobutene-derived dibromide with ethyl isocyanoacetate as the key step, followed by hydrolysis and subsequent acetylation. This methodology is generalized in order to prepare various linearly and angularly fused indane-based alpha-amino acid derivatives.
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