期刊
SYNTHESIS-STUTTGART
卷 -, 期 22, 页码 3897-3904出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0029-1217067
关键词
lactams; arylboronic acids; stannanes; Suzuki-Miyaura coupling; Stille coupling; resin-bound enol phosphinate
资金
- EPSRC
- GlaxoSmithKline
Enol phosphinates and phosphonates can be readily prepared from simple lactams in high yields and are both stable and storable. Both these substrates can be employed successfully in homogeneous Suzuki-Miyaura and Stille cross-couplings protocols. Additionally, the phosphonate group can be immobilised on a phenol-on-polystyrene resin and utilised in a simple diversity linker strategy in which the coupled product is cleaved from the resin under Suzuki-Miyaura cross-coupling conditions.
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