期刊
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY
卷 43, 期 2, 页码 131-134出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/15533174.2012.680090
关键词
CuFe2O4; magnetic properties; nanoparticles; X-ray diffraction
资金
- Fund of Weinan Teachers University [08YKZ008]
- Fund of Shaanxi Provincial Department of Education [12JK435]
CuFe2O4 nanoparticles have been obtained by heat treatment of coprecipitation product, which were synthesis by reaction of Cu2+ ions and Fe3+ in alkaline condition. The morphology and microstructure of the synthesized urchin-like superstructures have been characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The results show that the CuFe2O4 nanoparticles were polycrystal with cubic jacobsite structure and a size distribution from 20 to 40 nm. Magnetic properties have been detected by a vibrating sample magnetometer at room temperature. The nanoparticles exhibited a ferromagnetic behavior with the coercive force (Hc) value of 86.83Oe, saturation magnetization (Ms) value of 37.98 emu/g and remanent magnetization (Mr) value of 2.68 emu/g. The IR spectrum of peak at 586 cm-1 was corresponding to the vibration modes of CuFe2O4 nanoparticles.
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