期刊
SYNLETT
卷 24, 期 20, 页码 2695-2700出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0033-1340010
关键词
N-oxide reduction; tetrahydroxydiboron; selective reduction; in situ reduction; pyridine
Pyridine-N-oxides are often used as reactive precursors in the syntheses of substituted pyridines. Isolation and subsequent reduction of the associated pyridine-N-oxide intermediates can be challenging. We have discovered that tetrahydroxydiboron functions as a mild, versatile, and remarkably selective reducing agent for pyridine-N-oxides and may be used in an in situ fashion, thus obviating the isolation of N-oxide-containing intermediates
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