期刊
RSC ADVANCES
卷 5, 期 130, 页码 107829-107832出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ra24926k
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资金
- BBSRC [BB/F011539/1] Funding Source: UKRI
- EPSRC [EP/L011999/1] Funding Source: UKRI
- Biotechnology and Biological Sciences Research Council [BB/F011539/1] Funding Source: researchfish
- Engineering and Physical Sciences Research Council [EP/L011999/1] Funding Source: researchfish
The easy-to-interpret and rapid SelEXSIDE NMR experiment for measuring long-range H-1-C-13 scalar coupling constants nJCH is improved with increased sensitivity and resolution by the incorporation of 'pure-shift' homonuclear decoupling and IMPRESS-Hadamard encoding, with typical increases in signal-to-noise of over 300% and 400% demonstrated for small molecule examples, and narrower linewidths enabling measurement of smaller coupling constants.
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