期刊
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY
卷 49, 期 7, 页码 986-994出版社
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S1070428013070051
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资金
- Russian Foundation for Basic Research [11-03-97024-r_povolzh'e_a]
- Federal Grant-in-Aid Program Human Capital for Science and Education in Innovative Russia [14.740.11.0367]
Oxiranyl-substituted cycloalkenecarbonitriles obtained by the Beckmann fragmentation of oximes derived from levoglucosenone adducts with 1,3-butadiene, isoprene, cyclohexadiene, and cyclopentadiene were subjected to Red-Al reduction with opening of the epoxide ring. The reactions with 1,3-butadiene, isoprene, and cyclohexadiene derivatives were accompanied by cyclopropane ring closure and reduction of the cyano group to aldehyde, whereas the cyclopentadiene derivative underwent hydrogenolysis of the oxirane fragment.
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