期刊
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
卷 56, 期 11, 页码 1681-1687出版社
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0036023611110258
关键词
-
资金
- Chemistry and Materials Science Division
- Presidium of the Russian Academy of Sciences [OKh2.1, 27P3]
- [MK-305.2009.3]
Nanocrystalline powders of super-refractory complex carbides Ta4HfC5 and Ta4ZrC5 were synthesized using a hybrid method comprising sol-gel technology for preparing highly dispersed metal oxidescarbon starting mixtures and a relatively low-temperature (1300-1500A degrees C) carbothermal synthesis under a dynamic vacuum (P = 1 x 10(-3) to 1 x 10(-5) MPa). The elemental and phase compositions of the products and average crystallite sizes were determined. TEM was used to study particle morphology and dispersion. Microstructures were observed by SEM. BET specific surface areas were determined for powders prepared at 1400A degrees C.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据