期刊
RESEARCH ON CHEMICAL INTERMEDIATES
卷 36, 期 4, 页码 383-387出版社
SPRINGER
DOI: 10.1007/s11164-010-0148-z
关键词
3-Acetyl-6-(o-methylbenzoyl)-N-ethylcarbazole; Acylation; Aluminum chloride
资金
- National Natural Science Foundation of China [20776127]
- National Key Technology RD Program [2007BAI34B07]
- Zhejiang Province Science and Technology Program [2008C01006-1]
3-Acetyl-6-(o-methyl benzoyl)-N-ethylcarbazole was prepared through successive o-methyl benzoylation and acetylation of N-ethylcarbazole in one pot. The overall yield was 85.6% and the structure was confirmed by (1)H-NMR and (13)C-NMR. A preliminary investigation had also been carried out on the mechanism of the o-methyl benzoylation of N-ethylcarbazole.
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