期刊
POWDER TECHNOLOGY
卷 190, 期 1-2, 页码 95-98出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.powtec.2008.04.054
关键词
Spray-pyrolysis; Nano-powders; Boehmite; Alumina; Sol-gel
Boehmite (gamma-AlOOH) synthesis have been investigated using a spray pyrolysis (SP) device starting from a stable sol of Al-tri-sec-butoxide peptized by nitric acid. Free spherical particles from 100 to 500 nm have been elaborated. Particles sub-structure is made of nano-crystalline boehmite with very small average crystallite size (one crystal cell along the b axis). The nano-crystalline boehmite synthesized by SP at low temperature (200 degrees C) is spontaneously dispersible in water without any surface treatment. Boehmite powder may be transformed to transition gamma-alumina by heat post-treatment. Powders of sub-micrometric and spherical gamma-alumina particles may also be synthesized by SP at 700 degrees C. (C) 2008 Elsevier B.V. All rights reserved.
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