期刊
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
卷 186, 期 2, 页码 220-224出版社
TAYLOR & FRANCIS LTD
DOI: 10.1080/10426507.2010.492366
关键词
Catalyst-free; grinding; one-pot; solvent-free; thiazoles
资金
- National Key Technology RD Program [2007BAI34B00]
- Natural Science Foundation of Zhejiang Province [Y4080107]
An efficient and facile synthesis of 2,4-disubstituted thiazoles is achieved by a one-pot reaction of aldehydes and alpha-bromoketones with thiosemicarbazide by grinding under catalyst-and solvent-free conditions. This method has notable advantages in terms of simple workup, neat conditions, high yield, reasonably rapid reaction rate, and environmental friendliness.
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