4.1 Article

Solution and Crystal Structure of a Hexacoordinate Phosphoranate Bearing Two Martin Ligands and Two Methyl Groups

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TAYLOR & FRANCIS LTD
DOI: 10.1080/10426500902718265

关键词

Hexacoordinate; hypervalent; phosphorus; X-ray analysis

资金

  1. Ministry of Education, Culture, Sports, Science and Technology, Japan [14340199, 17350021]

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A hexacoordinate phosphoranate bearing two Martin ligands and two methyl groups was synthesized by the reaction of the monocyclic phosphorane bearing a hydroxy group with KH, and was crystallized in the presence of 18-crown-6 ether. The crystal structure of the phosphoranate could be regarded as an intermediate model in the reaction of the O-equatorial methylphosphorane with a methyl anion.

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