期刊
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
卷 184, 期 4, 页码 928-935出版社
TAYLOR & FRANCIS LTD
DOI: 10.1080/10426500902718265
关键词
Hexacoordinate; hypervalent; phosphorus; X-ray analysis
资金
- Ministry of Education, Culture, Sports, Science and Technology, Japan [14340199, 17350021]
A hexacoordinate phosphoranate bearing two Martin ligands and two methyl groups was synthesized by the reaction of the monocyclic phosphorane bearing a hydroxy group with KH, and was crystallized in the presence of 18-crown-6 ether. The crystal structure of the phosphoranate could be regarded as an intermediate model in the reaction of the O-equatorial methylphosphorane with a methyl anion.
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