4.6 Article

High Conversion, Solvent Free, Continuous Synthesis of Imidazolium Ionic Liquids In Spinning Tube-in-Tube Reactors

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ORGANIC PROCESS RESEARCH & DEVELOPMENT
卷 13, 期 1, 页码 64-66

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AMER CHEMICAL SOC
DOI: 10.1021/op8001917

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  1. Oak Ridge Institute for Science and Education (ORISE)
  2. United States Environmental Protection Agency
  3. Cooperative Research and Development Agreement [0252-03]

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A spinning tube-in-tube (STT) reactor has been used for the accelerated solvent-free synthesis of a number of 1-methylmidazole-based ionic liquids with excellent conversions (> 99%) and high throughputs (tens of kg/day).

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