期刊
ORGANIC LETTERS
卷 16, 期 9, 页码 2518-2521出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol500894k
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资金
- Natural Sciences and Engineering Research Council of Canada
- Alberta Glycomics Centre
- Alberta Innovates Technology Futures
A two-step route for introducing methyl phosphoramidate moieties onto carbohydrates is reported. The approach uses methyl pivolyl H-phosphonate as the phosphorylating reagent to produce an isolable carbohydrate H-phosphonate intermediate that is then oxidized by a Todd-Atherton reaction. The stability of the product methyl phosphoramidates was subsequently evaluated using various deprotection strategies.
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