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卷 16, 期 2, 页码 600-603出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol403504z
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- SFI
- UCD's School of Chemistry and Chemical Biology
A mild and rapid (diacetoxyiodo)benzene-mediated formal electrophilic alpha-azidation of 1,3-dicarbonyl compounds using commercially available Bu4NN3 as the azide source is reported. The reaction conditions employed are based on optimization studies conducted on the analogous halogenations with Et4NX (X = Cl, Br, 1).
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