期刊
ORGANIC LETTERS
卷 14, 期 17, 页码 4634-4637出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol302077n
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资金
- NIH [R01GM071779, P41GM081282]
- NSF [CHE-1048804]
- Division Of Chemistry
- Direct For Mathematical & Physical Scien [1048804] Funding Source: National Science Foundation
The total synthesis of the indole alkaloid hirsutine has been achieved, with a key step being the application of our phosphine-catalyzed [4 + 2] annulation of an imine with ethyl alpha-methylallenoate. From commercially available indole-2-carboxaldehyde, the target was synthesized in 14 steps and 6.7% overall yield.
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