期刊
ORGANIC LETTERS
卷 14, 期 19, 页码 5010-5013出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol3021435
关键词
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资金
- Ministry of Education, Culture, Sports, Science and Technology, Japan
- Japan Society for the Promotion of Science (JSPS) [21390001, 23689001]
- Grants-in-Aid for Scientific Research [21390001, 23689001] Funding Source: KAKEN
A mild and user-friendly one-pot oxidative cleavage of vicinal diols to their corresponding (di)carboxylic acids using AZADOs and Phl(OAc)(2) is described. 1,2-Diols and 2,3-diols as well as 1,2,3-triol gave one- or two-carbon-unit-shorter carboxylic acids. Internal vicinal diols also smoothly underwent one-pot oxidative cleavage to afford the corresponding dicarboxylic acids. Cyclic vicinal diols are converted to their corresponding open-form dicarboxylic acids.
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