期刊
ORGANIC LETTERS
卷 13, 期 16, 页码 4272-4275出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol201620g
关键词
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资金
- National Natural Science Foundation of China [20972157]
- 973 Program [2009CB825300]
- Natural Science Foundation of Liaoning Province [20102225]
- CAS [DICP K2009D04]
An efficient palladium(0)-catalyzed, Cu(I)-mediated synthetic route to trisubstituted olefins and conjugate dienes has been developed via oxo directing Liebeskind-Srogl cross-coupling reactions of gem-dihaloolefin-type alpha-oxo ketene dithioacetals with aryl and alkenylboronic acids. The synthetic protocol has demonstrated rare examples of transition-metal-promoted transformations of ketene dithioacetals, providing a novel route to highly functionalized conjugate dienes.
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