期刊
ORGANIC LETTERS
卷 13, 期 24, 页码 6532-6535出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol2028256
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资金
- Japan Society for the Promotion of Science (JSPS)
- Suntory Institute for Bioorganic Research
- Daiko Foundation
- Nagoya University
- Grants-in-Aid for Scientific Research [20380067, 22780102] Funding Source: KAKEN
The total synthesis of polygalolide A was accomplished through intramolecular C-glycosylation of glucal modified with siloxyfuran. The siloxyfuran group and siloxy substituent at the C-3 position played crucial roles in allowing direct access to the highly substituted oxabicyclo[3.2.1] core skeleton with correct quaternary stereogenic centers.
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