期刊
ORGANIC LETTERS
卷 12, 期 3, 页码 468-471出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol902642z
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资金
- Ministero dell'Universita
- dell'Istruzion e della Ricerca (MIUR)-Roma
- Universita degli Studi di Urbino
A one-pot Cu(II)-catalyzed aza-Michael addition of trimethylsilyl azide to 1,2-diaza-1,3-dienes and Cu(I)-catalyzed 1,3-dipolar cycloaddition of in situ generated alpha-azidohydrazones with alkynes is reported. This process combining two consecutive steps with recycling of the catalyst (Cu(OAc)(2)center dot H2O) represents a useful protocol for the smooth synthesis of novel pyrazolone-triazole derivatives.
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