期刊
ORGANIC LETTERS
卷 10, 期 20, 页码 4637-4640出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol801935r
关键词
-
资金
- Swedish Research Council
A general and efficient method for the microwave-assisted formation of the C-P bond was developed. Using a prevalent palladium catalyst, Pd(PPh3)(4), a quantitative cross-coupling of various H-phosphonate diesters with aryl and vinyl halides was achieved in less than 10 min. The reactions occurred with retention of configuration at the phosphorus center and in the vinyl moiety. Using this protocol, several C-phosphonates, including those bearing nucleoside and cholesteryl moieties, were prepared in high yields.
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