期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 9, 期 14, 页码 5104-5108出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1ob05710c
关键词
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资金
- EPSRC
- University of Manchester
- EPSRC [EP/G015287/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/G015287/1] Funding Source: researchfish
A tag removal-cyclisation sequence is described that is initiated by reduction using a Sm(II) species and completed by a Sm(III) Lewis acid that is formed in an earlier stage. Therefore, the reaction cascade utilises both oxidation states of a samarium reagent in discrete steps and allows access to privileged, pyrrolidinyl-spirooxindole scaffolds and analogues inspired by the anti-cancer natural product spirotryprostatin A.
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