期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 9, 期 16, 页码 5655-5658出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1ob05567d
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Photooxygenation of (beta-keto)-2-substituted furans leads, in a one pot operation, to functionalized 3(2H)-furanones with good to excellent yields. This methodology was applied as a key-step to the concise and biomimetic synthesis of the sesquiterpene merrekentrone C. The precursor to merrekentrone C, keto difuran, was synthesized using a cross coupling of alpha-iodo-3-acetylfuran with an alkenyl furan under Fenton-type conditions.
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