期刊
MOLECULAR DIVERSITY
卷 15, 期 1, 页码 163-172出版社
SPRINGER
DOI: 10.1007/s11030-010-9237-6
关键词
Organotrifloroborates; Suzuki-Miyaura; Click chemistry; Chemoenzymatic synthesis
类别
资金
- FAPESP [07/59404-2]
- CNPq [300613/2007-5]
- ANII [FCE252-2009]
The palladium catalyzed cross-coupling reaction of phenyltrifluoroborate with a chemoenzymatically derived bromoazidoconduritol, combined with 1,3-dipolar cycloaddition, with a variety of alkynes is described. Fourteen new compounds were synthesized in moderate to good yields. The click chemistry reaction can be effected by using sodium ascorbate and CuSO4 center dot 5H(2)O as catalyst in toluene-H2O at room temperature.
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