期刊
MICROPOROUS AND MESOPOROUS MATERIALS
卷 120, 期 1-2, 页码 29-34出版社
ELSEVIER
DOI: 10.1016/j.micromeso.2008.08.056
关键词
Zeolite Beta; Combined micro-mesoporous; Sol-gel; No template; Quenching
Composite micro- and mesoporous materials are synthesized using zeolite Beta nanoparticles without the need for a structure directing agent to form the mesopores. This leads to important ecological and economical advantages. The influence of the way of cooling the aged nanoparticles solution on the formation of the composite materials has been studied. The materials have been characterized towards porosity by N-2-sorption, towards zeolitic properties by TGA, DRIFT, XRD and TEM, towards aluminium content by EPMA. All prepared structures possess zeolitic properties. However, the method of cooling down of the aged seeds leads to differences in the porosity and intensity of the zeolitic characteristics. (C) 2008 Elsevier Inc. All rights reserved.
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