期刊
MICROPOROUS AND MESOPOROUS MATERIALS
卷 111, 期 1-3, 页码 632-635出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.micromeso.2007.07.022
关键词
[Al]-SBA-16; PH-adjusting; acid sites; mesostructured silica; direct synthesis; Al-27-MAS-NMR; FTIR; CO adsorption
A novel SBA-16-related synthesis of mesostructured silica containing framework aluminum is reported here. This material was successfully synthesized using aluminum sulphate and the pH-adjusting method. The structural and porosity properties of this novel material were studied by X-ray diffraction and N-2 adsorption at 77 K. The Al insertion was determined by Al-27-MAS-NMR and the acidity was monitored by infrared spectroscopy of CO adsorption at 100 K. (C) 2007 Elsevier Inc. All rights reserved.
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