期刊
MICROCHIMICA ACTA
卷 176, 期 1-2, 页码 109-115出版社
SPRINGER WIEN
DOI: 10.1007/s00604-011-0702-4
关键词
alpha-Fe(2)O(3) nanoparticles; Double-stranded DNA; Pb(2+); Sensor
资金
- National Natural Science Foundation of China [20775002]
- Anhui Normal University
Shuttle-like Fe(2)O(3) nanoparticles (NPs) were prepared by microwave-assisted synthesis and characterized by scanning electron microscopy and X-ray diffraction. The NPs were immobilized on a glassy carbon electrode and then covered with dsDNA. The resulting electrode gives a pair of well-defined redox peaks for Pb(II) at pH 6.0, with anodic and cathodic peak potentials occurring at -0.50 V and -0.75 V (vs. Ag/AgCl), respectively. The amperometric response to Pb(II) is linear in the range from 0.12 to 40 nM, and the detection limit is 0.1 nM at a signal-to-noise ratio of 3. The sensor exhibits high selectivity and reproducibility.
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