Microstructure-Dependent Local Strain Behavior in Polycrystals through In-Situ Scanning Electron Microscope Tensile Experiments

Digital image correlation of laser-ablated platinum nanoparticles on the surface of a polycrystalline metal (nickel-based superalloy Ren, 88DT) was used to obtain the local strain behavior from an in-situ scanning electron microscope tensile experiment at room temperature. By fusing this information with crystallographic orientations from electron backscatter diffraction (EBSD), a subsequent analysis shows that the average maximum shear strain tends to increase with increasing Schmid factor. Additionally, the range of the extreme values for the maximum shear strain also increases closer to the grain boundary, signifying that grain boundaries and triple junctions accumulate plasticity at strains just beyond yield in polycrystalline Ren, 88DT. In-situ experiments illuminating microstructure-property relationships of this ilk may be important for understanding damage nucleation in polycrystalline metals at high temperatures.