期刊
MATERIALS RESEARCH INNOVATIONS
卷 16, 期 5, 页码 362-367出版社
MANEY PUBLISHING
DOI: 10.1179/143307512X13463991318033
关键词
Sol-gel; Metal-carbon xerogel; Nanoparticles; Magnetic materials
资金
- Doctoral Program Foundation of Liaoning Province [20091047]
Transition metal (Fe, Co and Ni) doped carbon xerogels (CXs) were synthesised by one-pot pyrolysis of the sol-gel polymer of resorcinol and formaldehyde in the presence of the corresponding metal nitrates. N-2 adsorption-desorption and scanning and transmission electron microscopies proved that the addition of different metals could exert a remarkable influence on the textural properties. From X-ray diffraction, the phase of the metallic species was confirmed. Scanning electron microscopy images revealed that the surface morphologies of the resultant metal-CXs were composed of carbon microspheres. Transmission electron microscopy observations illustrated that Ni-CX was made of uniform carbon nanotubes that differed from the core/shell structures of Fe-and Co-xerogels. Measurements on the magnetic properties indicated that the Fe-, Co- and Ni-CXs exhibited typical ferromagnetic characteristics at room temperature.
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