Fast preparation of Bi2GeO5 nanoflakes via a microwave-hydrothermal process and enhanced photocatalytic activity after loading with Ag nanoparticles

In this work, a facile and rapid microwave-assisted hydrothermal route has been developed to prepare Bi2GeO5 nanoflakes. Ag nanoparticles were subsequently deposited on the Bi2GeO5 nanoflakes by a photoreduction procedure. The phases and morphologies of the products were characterized by powder X-ray diffraction (XRD), X-ray photoelectron spectrum (XPS), transmission electron microscopy (TEM), scanning electron microscopy (SEM), and UV-vis diffuse reflectance spectroscopy. Photocatalytic experiments indicate that such Ag/Bi2GeO5 nanocomposite possesses higher photocatalytic activity for RhB degradation under UV light irradiation in comparison to pure Bi2GeO5. The amount of Ag in the nanocomposite affects the catalytic activity, and 3 wt% Ag showed the highest photodegradation efficiency. Moreover, the catalyst remains active after four consecutive tests. The present study provides a new strategy to design composite materials with enhanced photocatalytic activity. (C) 2012 Elsevier Ltd. All rights reserved.