期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 133, 期 27, 页码 10376-10378出版社
AMER CHEMICAL SOC
DOI: 10.1021/ja2042854
关键词
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资金
- National Institutes of Health [NIGMS P50-GM067082]
- National Science Foundation
The first stereoselective synthesis of epimeloscine has been accomplished in 13 total steps with a longest linear sequence of 10 steps. The core of the synthesis takes only five steps, the key ones being acylation, stereoselective tandem radical cyclization of a divinylcyclopropane to make two rings, and group-selective ring-closing metathesis of the resulting divinylcyclopentane to make the last ring.
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