4.2 Article

High-energy X-ray diffraction using the Pixium 4700 flat-panel detector

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JOURNAL OF SYNCHROTRON RADIATION
卷 16, 期 -, 页码 463-468

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INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S0909049509015519

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high-energy X-rays; flat-panel detector; Pixium detector; diffraction; large area detectors; detector noise; MAR image plate

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The Pixium 4700 detector represents a significant step forward in detector technology for high-energy X-ray diffraction. The detector design is based on digital flat-panel technology, combining an amorphous Si panel with a CsI scintillator. The detector has a useful pixel array of 1910 X 2480 pixels with a pixel size of 154 mm X 154 mm, and thus it covers an effective area of 294 mm X 379 mm. Designed for medical imaging, the detector has good efficiency at high X-ray energies. Furthermore, it is capable of acquiring sequences of images at 7.5 frames per second in full image mode, and up to 60 frames per second in binned region of interest modes. Here, the basic properties of this detector applied to high-energy X-ray diffraction are presented. Quantitative comparisons with a widespread high-energy detector, the MAR345 image plate scanner, are shown. Other properties of the Pixium 4700 detector, including a narrow point-spread function and distortion-free image, allows for the acquisition of high-quality diffraction data at high X-ray energies. In addition, high frame rates and shutterless operation open new experimental possibilities. Also provided are the necessary data for the correction of images collected using the Pixium 4700 for diffraction purposes. (C) 2009 International Union of Crystallography Printed in Singapore - all rights reserved

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