期刊
JOURNAL OF SOLID STATE CHEMISTRY
卷 211, 期 -, 页码 51-57出版社
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jssc.2013.12.004
关键词
HPW/MCM-48; Mesoporous materials; Green synthesis; Benzoic acid
资金
- National Natural Science Foundation of PR China [U1304203, J1210060]
- Innovation Foundation of Zhengzhou University [2013xjxm022]
MCM-48 and tungstophosphoric acid (HPW) were prepared and applied for the synthesis of HPW/MCM-48 mesoporous materials. The characterization results showed that HPW/MCM-48 obtained retained the typical mesopore structure of MCM-48, and the textural parameters decreased with the increase loading of HPW. The catalytic oxidation results of benzyl alcohol and benzaldehyde with 30% H2O2 indicated that HPW/MCM-48 was an efficient catalyst for the green synthesis of benzoic acid. Furthermore, 35 wt% HPW/MCM-48 sample showed the highest activity under the reaction conditions. (C) 2013 Elsevier Inc. All rights reserved.
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