期刊
JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
卷 62, 期 3, 页码 424-431出版社
SPRINGER
DOI: 10.1007/s10971-012-2744-4
关键词
Superhydrophobic; Titanium dioxide nanoparticles; Vinyltriethoxysilane; Polystyrene; Grafting
资金
- Scientific Research Foundation for the Returned Overseas Scholars in Jinan [20100406]
- Youth Scientist Fund of Shandong Province [BS2011CL025]
- Doctoral Startup Foundation of Shandong Polytechnic University
- National Natural Science Foundation of China [50902089, 51172132]
- Independent Innovation Foundation of Shandong University (IIFSDU) [2009JC012]
- Shandong Province Natural Science Foundation [ZR2010EM020]
The organic-inorganic nanocomposite films were fabricated by grafting polystyrene (PS) onto the vinyltriethoxysilane (VTEOS) modified titanium dioxide nanopowders using free radical polymerization. The composition of the surfaces and the structure for the PS grafted titania (PS-g-TiO2) were examined by infrared spectroscopy, X-ray photoelectron spectroscopy and thermogravimetric analysis, and the rough surface was confirmed by the evaluation of the morphological characteristics of the coating using hybrid particles. The wetting properties of the VTEOS modified titania and PS-g-TiO2 films were investigated, which show the maximum static water contact angles of 160A degrees and 154A degrees, and minimum sliding angles of 3A degrees and 4A degrees, respectively.
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