期刊
JOURNAL OF PHYSICAL CHEMISTRY C
卷 114, 期 20, 页码 9221-9226出版社
AMER CHEMICAL SOC
DOI: 10.1021/jp9114404
关键词
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资金
- National Basic Research Priorities Program [2007CB914100/3]
- National Natural Science Foundation of China [NSFC 20735005, NSFC20875017, NSFC 30873132]
- Technological Innovation Program of Shanghai [09JC1401100]
- Shanghai Leading Academic Discipline Project [B109]
In this work, we reported an alternative strategy to the synthesis of core-shell structure Fe3O4@C@Au magnetic microspheres by a self-assembly approach. The as-synthesized Fe3O4@C@Au magnetic microspheres were functionalized with 4-mercaptophenylboronic acid and successfully applied for selective enrichment of glycopeptides and glycoproteins. At first, the Fe3O4@C magnetic microspheres were synthesized by two-step reactions including solvothermal and hydrothermal reactions. Then. Fe3O4@C@Au magnetic microspheres with core-shell structure were obtained by a self-assembly approach. Finally, the Fe3O4@C@Au magnetic microspheres were modified with 4-mercaptophenylboronic acid. The 4-mercaptophenylboronic acid-modified Fe3O4@C@Au magnetic microspheres were successfully applied to selective enrichment of glycoproteins and glycopeptides.
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