期刊
JOURNAL OF PHYSICAL CHEMISTRY C
卷 112, 期 47, 页码 18426-18430出版社
AMER CHEMICAL SOC
DOI: 10.1021/jp802778p
关键词
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资金
- National Natural Science Foundation of China [50504017]
- Hunan Provincial Key Science and Technology Project of China [2007FJ3008]
- Hunan Postdoctoral Scientific Program of China [2006FJ4230]
- China Postdoctoral Science Foundation [20060400262]
Uniform single-crystalline indium hydroxide microcubes can be successfully synthesized in large quantities via a convenient hydrothermal route using hydrated indium nitrate and sodium borohydride as reagents under mild conditions. The morphology and size of indium hydroxide microcubes can be controlled by varying the synthetic parameters such as hydrothermal time, reaction temperature, and surfactant. Single-crystalline indium oxide microcubes also can be successfully prepared by a thermal decomposition method using indium hydroxide microcubes as the precursor. The phase structures, morphologies, and optical properties of the final products were investigated in detail by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, differential scanning calorimetric analysis, thermogravimetric analysis, and photoluminescence spectroscopy. These uniform single-crystalline microcubes may be useful in microelectronic and optoelectronic devices.
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