期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 79, 期 8, 页码 3684-3687出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo500336e
关键词
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A nonracemic synthesis of the glucolcinase-glucokinase regulatory protein disruptor AMG-3969 (5) is reported. Key features of the synthetic approach are an asymmetric synthesis of the 2-alkynyl piperazine core via a base-promoted isomerization and a revised approach to the synthesis of the aminopyridinesulfonamide with an improved safety profile.
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