期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 78, 期 17, 页码 8705-8711出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo401435v
关键词
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资金
- National Natural Science Foundation of China [21072148]
- Foundation (B) for Peiyang Scholar-Young Core Faculty of Tianjin University [2013XR-0144]
- Innovation Foundation of Tianjin University [2013XJ-0005]
Treatment of N-alkoxyamides with NBS in toluene was found to conveniently afford the corresponding carboxylic esters, including those bearing a bulky or long-chain substituent, in satisfactory to excellent yields. This approach not only represents a convenient and economic approach to a direct transformation of an alkoxyamide moiety into the carboxylic ester functional group, via oxidative homocoupling and the subsequent thermal denitrogenation, but also facilitates the synthesis of sterically hindered carboxylic esters.
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