期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 78, 期 8, 页码 3767-3773出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo400212u
关键词
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资金
- National Science Foundation [CHE-1009038, 1262479]
- Government of Russia (FCP) [GK11.519.11.5010]
- Government of Russia [Zayavka 2011-1.9-519-024-070, 2012-220-03-9803]
- Government of Russia (Russian Foundation for Basic Research) [12-03-00978-a]
- Direct For Mathematical & Physical Scien [1009038] Funding Source: National Science Foundation
- Division Of Chemistry [1009038] Funding Source: National Science Foundation
- Division Of Chemistry
- Direct For Mathematical & Physical Scien [1262479] Funding Source: National Science Foundation
Various 1-arylbenziodoxolones can be conveniently prepared from 2-iodobenzoic acid and arenes by a one pot procedure using Oxone (2KHSO(5)center dot KHSO4 center dot K2SO4) as an inexpensive and environmentally safe oxidant This procedure is also applicable for the synthesis of the 7-methylbenziodoxolone ring system using 2-iodo-3-methylbenzoic acid as starting compound. Structures of four 1-arylbenziodoxolone derivatives were established by single crystal X-ray diffraction analysis. An enhanced reactivity of 1-aryl-7-methylbenziodoxolones toward nucleophiles compared to unsubstituted 1-arylbenziodoxolones has been found.
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