期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 78, 期 24, 页码 12809-12813出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo402220s
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资金
- German Research Foundation DFG
An efficient, robust, and scalable synthesis of an azido precursor to the modified amino acid (2S,5R)-5-hydroxylysine was developed on the basis of the use of a highly stereoselective organocatalytic alpha-chlorination-reduction protocol. The final Fmoc-protected (2S,5R)-6-azido-5-hydroxylysine derivative can be used in solid-phase peptide synthesis, providing access to proteins that contain large quantities of post-translationally modified lysine (e.g., collagens).
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