期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 78, 期 15, 页码 7749-7753出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo401099e
关键词
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资金
- ETH Zurich
- ETH Independent Investigator's Research Award
- Carlsberg Foundation
The (trifluoromethyl)stannane reagent, Bu3SnCF3, was found to react under CsF activation with ketones and aldehydes to the corresponding trifluoromethylated stannane ether intermediates at room temperature in high yield. Only a mildly acidic extraction (aqueous NH4Cl) is required to release the corresponding trifluoromethyl alcohol products. The protocol is compatible with acid-sensitive functional groups.
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