期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 76, 期 10, 页码 4071-4074出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo102406j
关键词
-
资金
- National Natural Science Foundation of China [20902084]
- Science and Technology Office in Zhejiang Province [2010R10016]
- Zhejiang Normal University
A highly regio- and stereoselective method for the synthesis of cis-1,2-dihaloalkenes through Pd-catalyzed coupling of haloalkynes and alpha, beta-unsaturated carbonyls has been reported. Excellent stereoselectivities (Z/E up to > 98:2) were observed in most cases. This method was subsequently applied to synthesize the functionalized conjugated enyne via the mono-Sonogashira coupling reaction of cis-1-chloro-2-iodoalkene.
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